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    The spent electrolyte was oxidised with the cell sludge as well as additional manganese ore in which manganese must be present in a valence greater than 2. 2. After digestion, the pH was adjusted to 5.5?.0 to precipitate Fe and some of Mo as sludge. 3. The pH was then adjusted to 7.0?.5 and (NH 4) 2 S added to precipitate the Mo, Co, and Ni.

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    The spent electrolyte was oxidised with the cell sludge as well as additional manganese ore in which manganese must be present in a valence greater than 2. 2. After digestion, the pH was adjusted to 5.5?.0 to precipitate Fe and some of Mo as sludge. 3. The pH was then adjusted to 7.0?.5 and (NH 4) 2 S added to precipitate the Mo, Co, and Ni.

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